Adding a certain compound to certain chemical reactions, such as: 94-46-2, name is Isoamyl Benzoate, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 94-46-2, Safety of Isoamyl Benzoate
Trifluoromethylthio silver (0.5 mmol), 2,6-lutidine (0.1 mmol) and ammonium persulfate (1.0 mmol) were added to the reaction flask, and after evacuating the argon three times, isoamyl benzoate 1.0 mmol) and acetonitrile (5 mL). The reaction flask was placed in an oil bath at 90 C start heating and stirring 2h removed, to be cooled to room temperature. Using trifluoromethylbenzene as an internal standard substance, it was confirmed by 19F-NMR that 3-methyl-3-trifluoromethylthiobutyl benzoate was formed (a yield of 63%). The reaction mixture was filtered and the filtrate was evaporated to remove the solvent by a rotary evaporator. The residue was separated by column chromatography and concentrated under reduced pressure to give a colorless oil (75 mg, yield 51%).
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Reference:
Patent; Chinese Academy Of Sciences Shanghai Organic Chemistry Institute; Chen Qingyun; Liu Chao; Wu Hao; Xiao Zhiwei; (15 pag.)CN104557358; (2017); B;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics