Category: 72338-48-8

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 72338-48-8, name is Ethyl 12-bromododecanoate, This compound has unique chemical properties. The synthetic route is as follows., COA of Formula: C14H27BrO2

c) Synthesis of ethyl 13-(diethoxyphosphoryl)tridecanoate In a single-neck flask with a reflux condenser, ethyl 12-bromododecanoate is weighed (1.8 g, 7.37 mmol) and triethyl phosphite (2.6 mL, 15 mmol) is added. The reaction mixture is brought to 150C and left stirring under a static head of nitrogen. After 24 hours the one neck balloon is attached to the high vacuum pump to eliminate volatile products and the resulting dense oil is directly loaded with column chromatography on silica gel. It is eluted with a mixture of ethyl acetate/petroleum ether 1/1 which leads to the isolation of 2.5 g (yield 94%) of ethyl 13-(diethoxyphosphoryl)tridecanoate as a colourless oil.

According to the analysis of related databases, 72338-48-8, the application of this compound in the production field has become more and more popular.

Reference:
Patent; Colorobbia Italia S.p.a.; EP1979365; (2012); B1;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics

In the chemical reaction process, reaction time, type of solvent, can easily affect the result of the reaction, thereby determining the yield and properties of the reaction product. An updated downstream synthesis route of 72338-48-8 as follows. category: esters-buliding-blocks

2.98 g of amantadine was dissolved in 15 mL of DMF, and 5.5 g of ethyl bromododecanoate and 4.9 g of K2CO3 were added.Reaction at 60 C for 16 hours;Then diluted with 100 mL of water and extracted with ethyl acetate (3¡Á50 mL);After the organic phase is combined, it is dried with sodium, and then the solid is filtered off.The filtrate is concentrated in vacuo and purified to give a yellow oil, 12-(adamantyl)aminododecanoate;

According to the analysis of related databases, 72338-48-8, the application of this compound in the production field has become more and more popular.

Reference:
Patent; China Agricultural University; Wang Zhanhui; Jiang Haiyang; Wen Kai; Shen Jianzhong; Zhang Xiya; Chen Chaochao; Duan Changfei; Yu Wenbo; Yu Xuezhi; (17 pag.)CN110105232; (2019); A;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics