Category: 4720-83-6

Simple exploration of 4720-83-6

Adding a certain compound to certain chemical reactions, such as: 4720-83-6, name is 6-Oxabicyclo[3.2.1]oct-3-en-7-one, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 4720-83-6, HPLC of Formula: C7H8O2

Adding a certain compound to certain chemical reactions, such as: 4720-83-6, name is 6-Oxabicyclo[3.2.1]oct-3-en-7-one, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 4720-83-6, HPLC of Formula: C7H8O2

Step 3: To a stirred solution of alkene intermediate (1 .68 g, 13.50 mmol, 1 equiv.) in dry THF (70 mL), was added dropwise lithium aluminum hydride (1 M in THF, 20 ml_, 20 mmol, 1 .5 equiv.) at 0C under azote atmosphere. The reaction mixture was kept at 0C for 1 hours. Then, water (2 ml_), 15% aqueous sodium hydroxide (2 mL) and water (5 mL) were successively added, and the mixture was allowed to warm to room temperature and stirred for 2h30. The salts were filtered through a pad of celite and the filtrate was dried over Na2S04 and concentrated under vacuum to yield (1 S,5S)-5-(hydroxymethyl)cyclohex-2-en-1 -ol (1 .87 g, quant.) as a colorless oil.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 6-Oxabicyclo[3.2.1]oct-3-en-7-one, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; BCI PHARMA; SURLERAUX, Dominique; AMIABLE, Claire; GUILLON, Remi; (239 pag.)WO2017/191297; (2017); A1;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics

The important role of 4720-83-6

Reference of 4720-83-6, These common heterocyclic compound, 4720-83-6, name is 6-Oxabicyclo[3.2.1]oct-3-en-7-one, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

Reference of 4720-83-6, These common heterocyclic compound, 4720-83-6, name is 6-Oxabicyclo[3.2.1]oct-3-en-7-one, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

To 6-oxabicyclo [3.2. 1] oct-3-en-7-one (2.6 g, 21 mmol) in xylenes (50 ml) under nitrogen was added benzylamine (3.42 g, 32 mmol). The mixture was heated under reflux for 16 h, then cooled to room temperature. The heavy white precipitate was collected by filtration, and recrystallized from dichloromethane/hexane to give the amide as a white solid (3.8 g, 78%, m. p. 127- 128C)

The synthetic route of 4720-83-6 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; TARGACEPT, INC.; WO2005/37832; (2005); A2;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics