Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 2521-91-7, name is Ethyl 2-((3-bromophenyl)amino)acetate, This compound has unique chemical properties. The synthetic route is as follows., Formula: C10H12BrNO2
General procedure: A mixture of sodium methoxide (10 mmol) and hydroxylaminehydrochloride (6 mmol) in anhydrous methanolwaswell stirred for30 min. To this mixture was added compound 5 or 6 (3 mmol) wasadded, and the mixture was stirred at room temperature for 1-3 h.The reaction was quenched with ice (30 g) and neutralized withdilute HCl, which was extracted with ethyl acetate (3 60 mL). Theorganic layers were collected, dried over sodium sulfate, filtered,and evaporated under vacuum. The residure was purified by flashsilica chromatography (methanol-dichloromethane) to afford pureproduct (2 or 3) as a white solid.
According to the analysis of related databases, 2521-91-7, the application of this compound in the production field has become more and more popular.
Reference:
Article; Liu, Qi; Shi, Wei-Kang; Ren, Shen-Zhen; Ni, Wei-Wei; Li, Wei-Yi; Chen, Hui-Min; Liu, Pei; Yuan, Jing; He, Xiao-Su; Liu, Jia-Jia; Cao, Peng; Yang, Pu-Zhen; Xiao, Zhu-Ping; Zhu, Hai-Liang; European Journal of Medicinal Chemistry; vol. 156; (2018); p. 126 – 136;,
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