The important role of 1127-01-1

The chemical industry reduces the impact on the environment during synthesis Ethyl 1-hydroxycyclohexanecarboxylate. I believe this compound will play a more active role in future production and life.

Synthetic Route of 1127-01-1, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 1127-01-1, name is Ethyl 1-hydroxycyclohexanecarboxylate, This compound has unique chemical properties. The synthetic route is as follows.

2,09 g 1-HYDROXYCYCLOHEXANCARBONSaeURE-ETHYLESTER und 3 g der Verbindung gemaess Beispiel XXIV-1 werden im Oelbad auf 120C erhitzt und bis zum Ende der Gasentwicklung verruehrt und dann noch kurz auf 140C erhitzt. Ausbeute : 42 g (59 % der Theorie). 1H-NMR (400 MHz, CD3CN) : No. = 2,58 (q, 2H, CH2-AR), 3,77 (s, 3H, OCH3), 4,05 (m, 2H, O- CH2-CH3) ppm.

The chemical industry reduces the impact on the environment during synthesis Ethyl 1-hydroxycyclohexanecarboxylate. I believe this compound will play a more active role in future production and life.

Reference:
Patent; BAYER CROPSCIENCE AKTIENGESELLSCHAFT; LUBOS-ERDELEN, Angelika; WO2004/80962; (2004); A1;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics

The important role of 1127-01-1

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of Ethyl 1-hydroxycyclohexanecarboxylate.

Adding some certain compound to certain chemical reactions, such as: 1127-01-1, name is Ethyl 1-hydroxycyclohexanecarboxylate, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 1127-01-1. 1127-01-1

1. Preparation of Hexylester: Example 1a with Modification (Column 125) 0.1 mol of ethyl-1-hydroxycyclohexanecarboxylate were introduced into 200 ml of absolute methylene dichloride, 0.12 mol of triethylamine (Et3N) were added, and a solution of 0.1 mol of 2-(2,4-dichlorophenyl)acetyl chloride in 50 ml of absolute methylene dichloride was added dropwise at 0-10 C. After the solution had been stirred for 16 h at room temperature, it was washed with aqueous citric acid and aqueous sodium bicarbonate solution, and the organic phase was dried over sodium sulfate and evaporated on a rotary evaporation.

Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of Ethyl 1-hydroxycyclohexanecarboxylate.

Reference:
Patent; ROTAM AGROCHEM INTERNATIONAL COMPANY LIMITED; BRISTOW, James Timothy; (13 pag.)US2017/166546; (2017); A1;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics