Adding a certain compound to certain chemical reactions, such as: 111-61-5, name is Ethyl stearate, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 111-61-5, Quality Control of Ethyl stearate
Reaction experiments were carried out in a 50 ml stainless steelautoclave. All the catalysts were pre-reduced in hydrogen at tem-perature (150, 200, 500C) for 90 min before the reaction. Afterreduction, the catalyst was transferred into the autoclave, in which5.0 ml hexane was added as solvent, under the protection of hydro-gen. After that, a certain amount of ethyl stearate was added andthe autoclave was sealed. The reaction was operated under a stir-ring rate of 1300 rpm (without diffusion limitation) at 230C and aH2pressure of 3.0 MPa H2. After the reaction for several hours, the autoclave was cooled to room temperature. The products were col-lected and then analyzed by gas chromatography with FID detectorwith a DB-1 capillary column and GC-MS.
At the same time, in my other blogs, there are other synthetic methods of this type of compound, Ethyl stearate, and friends who are interested can also refer to it.
Reference:
Article; He, Limin; Li, Xiaoru; Lin, Weiwei; Li, Wei; Cheng, Haiyang; Yu, Yancun; Fujita, Shin-Ichiro; Arai, Masahiko; Zhao, Fengyu; Journal of Molecular Catalysis A: Chemical; vol. 392; (2014); p. 143 – 149;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics