Synthetic Route of 36692-49-6, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 36692-49-6, name is Methyl 3,4-diaminobenzoate, This compound has unique chemical properties. The synthetic route is as follows.
General procedure: In 25 ml round-bottomed flask, a mixture of 1,2-phenylendiamine (1 mmol), a-bromoacetophenone(1 mmol) and BAILnano-SiO2 catalyst (35 mol%) was preparedand the reaction mixture was stirred at room temperature for the time shown inTable 2. The progress of the reaction was monitored by TLC. After completion of the reaction, ethyl acetate (5 mL) was added and the catalyst was separated by simplefiltration. The residue was dried over anhydrous Na2SO4 and after evaporation ofsolvent the pure product was obtained by recrystallization from ethanol.
The chemical industry reduces the impact on the environment during synthesis Methyl 3,4-diaminobenzoate. I believe this compound will play a more active role in future production and life.
Reference:
Article; Daragahi, Seyed Arash Hosseini; Mohebat, Razieh; Mosslemin, Mohammad Hossein; Organic Preparations and Procedures International; vol. 50; 3; (2018); p. 301 – 313;,
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