An article Pd-Colloids-Catalyzed/Ag2O-Oxidized General and Selective Esterification of Benzylic Alcohols WOS:000473713900001 published article about AEROBIC OXIDATIVE ESTERIFICATION; LIGAND-FREE PALLADIUM; CARBOXYLIC-ACIDS; CATALYZED SYNTHESIS; TERMINAL ALKYNES; HIGHLY EFFICIENT; HECK REACTION; ALDEHYDES; NANOPARTICLES; ESTERS in [Sable, Vaibhav; Shah, Jagrut; Sharma, Anuja; Kapdi, Anant R.] Inst Chem Technol, Dept Chem, Nathalal Parekh Rd, Mumbai 400019, Maharashtra, India in 2019.0, Cited 85.0. Application In Synthesis of Methyl 3-phenyl-2-propenoate. The Name is Methyl 3-phenyl-2-propenoate. Through research, I have a further understanding and discovery of 103-26-4
Palladium colloids obtained from the degradation of Hermann-Beller palladacycle proved to be an efficient catalytic system in combination with silver oxide as a selective oxidant for the oxidative esterification of differently substituted benzyl alcohols in MeOH as solvent. Excellent reactivity exhibited by the catalytic system also allowed the alcoholic coupling partner to be changed from MeOH to a wide range of alcohols having diverse functionalities. The mildness of the developed protocol also made it possible to employ propargyl alcohol as the coupling partner without any observation of any interference of the terminal alkyne. Selective oxidative coupling of a primary alcoholic functional group over secondary in the case of glycols and glycerols was also made possible using the developed catalyst system. To test the relevancy of Pd/Ag combined catalysis mixed Pd/Ag colloids were synthesized, characterized by TEM, XRD and XPS and applied to oxidative-esterification successfully.
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Reference:
Article; Weng, Shiue-Shien; Ke, Chih-Shueh; Chen, Fong-Kuang; Lyu, You-Fu; Lin, Guan-Ying; Tetrahedron; vol. 67; 9; (2011); p. 1640 – 1648;,
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