Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 50413-30-4, name is Methyl 2-amino-4-methoxylbenzoate, This compound has unique chemical properties. The synthetic route is as follows., Safety of Methyl 2-amino-4-methoxylbenzoate
Example 1 : methyl 4-methoxy-2-[(3-UQ-methgammal-lH-imidazol-4-yl)sulfonyllamino} quinoxalin-2-yl)aminolbenzoate; N-(3-chloroquinoxalin-2-yl)-l -methyl- lH-imidazole-4-sulfonamide (2 g; 6.2 mmol; 1 eq) and methyl 2-amino-4-methoxybenzoate (1.2 g; 6.8 mmol; 1.1 eq) are taken up in water (60 mL) and acetic acid (160 muL; 3.65 mmol; 0.6 eq) is added. The suspension is heated up to 1700C in the microwave under normal absorption for 20 min. The reaction is stopped by filtration of the solid and washing with water until neutral. The orange powder obtained is dried under vaccum at 400C overnight then taken up in DCM. Triethylamine (1.72 mL) is added. After sonication, the solvents are removed under reduced pressure and the residue obtained is washed with water then dried under vacuum at 400C overnight. The powder is taken up in MeOH and refluxed then the suspension is left at 4C for Ih. The precipitate is filtered and washed with MeOH then dried under vacuum at 4O0C for 2 days, to afford 1.68 g (58%) of the title compound as a yellow
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 50413-30-4.
Reference:
Patent; LABORATOIRES SERONO SA; WO2008/101979; (2008); A1;,
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