Application of 2475-80-1, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 2475-80-1, name is Methyl 2-amino-5-methoxybenzoate, This compound has unique chemical properties. The synthetic route is as follows.
Methyl 2-amino-5- (methyloxy) benzoate (20.22 g, 0.112 mol) was dissolved in toluene in a 500 mL single neck flask,Triethylamine (22.58 g, 0.223 mol) was addedIsopropylsulfamoyl chloride (16.82 g, 0.117 mol),80 reaction 1h.The reaction was completed, extracted with water, the organic phase was collected, the aqueous phase was extracted with ethyl acetate, the combined organic phase was washed with saturated sodium bicarbonate,And dried over anhydrous sodium sulfate,The solvent was distilled off under reduced pressure to give 29.50 g of methyl 5- (methyloxy) -2 – ((N-isopropylsulfonyl) amino) benzoate in a yield of 91.7%.
The chemical industry reduces the impact on the environment during synthesis Methyl 2-amino-5-methoxybenzoate. I believe this compound will play a more active role in future production and life.
Reference:
Patent; Guizhou University; Yue Yi; Zhao Chunshen; Zhou Zhixu; Liu Li; Huang Zhuyan; Teng Minggang; (14 pag.)CN106478548; (2017); A;,
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