Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 2672-58-4, name is Trimethyl benzene-1,3,5-tricarboxylate, This compound has unique chemical properties. The synthetic route is as follows., Product Details of 2672-58-4
Synthesis of 1,3,5-Tris(hydroxymethyl)benzene (50)(Y. Yamaqiwa, Y. Koreishi. S. Kivozumi, M. Kobavashi, T. Kamikawa, M. Tsukino, H. Goi M. Yamamaoto, M. Munakata. Bull. Chem. Soc. Jpn. 1996, 69, 3317-3323; J. Houk, G. Whitesides. J. Am. Chem. Soc. 1987, 109, 6825-6836) A solution of 1,3,5-tris(methoxycarbonyl)benzene (10.09 g, 40 mmol) in dry THF (400 ml) was added over a period of 3h to a suspension of LiAlH4 (4.03 g, 0.1 mol) in dry THF (300 ml) under N2. After stirring over night at room temperature, the reaction mixture was cooled to 0 C., hydrolyzed with water (4 ml), 2M NaOH (4 ml) and water (12 ml), filtered, and the filter cake washed thoroughly with THF. The combined filtrates were concentrated and the crude product was recrystallized from hot (not boiling) ethanol to afford 50(5.59 g, 83%) as white needles; mp 76-77 C. (lit. 77-78 C.) 1H NMR (300 MHz, DMSO-d6) delta4.49 (d, 3H, J4.8 Hz, CH2), 5.30 (t, 1H, J5.4 Hz, OH), 7.14 (s, 1H, aromat. H).
According to the analysis of related databases, 2672-58-4, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Davis, Benjamin G.; Jones, John Bryan; Bott, Richard R.; US2002/19039; (2002); A1;,
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