Qualitative and semi-quantitative analysis of specific aroma in Ampelopsis grossedentata based on HS-SPME/GC-MS was written by Shen, Dong;Shen, Qiang;Pan, Ke;Zheng, Wen-jia. And the article was included in Guizhou Nongye Kexue in 2010.Synthetic Route of C15H22O2 The following contents are mentioned in the article:
The specific aroma components of Ampelopsis grossedentata were qual. and semi-quant. analyzed by HS-SPME/GC-MS based on optimization of sample dosage, extraction temperature, extraction time, balanced time and desorption time to provide theor. basis for further development of Ampelopsis grossedentata. The results showed that the optimum HS-SPME conditions were 0.5 g sample dosage, 50°C, 50 min extraction time, 10 min balanced time, 2.5 min absorption time. The specific aroma components were nonanal, decanal, cis-geranylacetone, 6,10,14-trimethyl-2-pentadecanone, di-Et phthalate, phthalic acid, diisobutyl ester, 2,6-bis(1,1-dimethylethyl)-4-methyl-phenol, 2,4-bis(1,1-dimethylethyl)-phenol, β-ionone, 1,1,3-trimethyl-3-phenyl-indane and (R)-5,6,7,7a-tetrahydro-4,4,7a-trimethyl-2(4H)-benzofuranone. The HS-SPME/GC-MS with less sample dosage, reliability, simplicity and rapidity can be used in qual. and semi-quant. anal. of Ampelopsis grossedentata specific aroma components. This study involved multiple reactions and reactants, such as 2-Ethylhexyl benzoate (cas: 5444-75-7Synthetic Route of C15H22O2).
2-Ethylhexyl benzoate (cas: 5444-75-7) belongs to esters. Esters are widespread in nature and are widely used in industry. In nature, fats are in general triesters derived from glycerol and fatty acids. Esters are responsible for the aroma of many fruits. Cyclic esters are called lactones, regardless of whether they are derived from an organic or inorganic acid. One example of an organic lactone is γ-valerolactone.Synthetic Route of C15H22O2
Referemce:
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics