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Iron-catalyzed carbonylative cyclization of gamma,delta-unsaturated aromatic oxime esters with amines
An efficient iron-catalyzed carbonylative cyclization of gamma,delta-unsaturated aromatic oxime esters with amines has been developed. A range of functionalized beta-homoproline amide derivatives were prepared via an iminyl radical-mediated intramolecular 1,5-cyclization followed by carbon radical-triggered intermolecular carbonylation. Examples on further transforming the obtained product were successfully discussed as well.
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