Related Products of 17100-65-1, A common heterocyclic compound, 17100-65-1, name is Methyl 2-bromo-4-methoxybenzoate, molecular formula is C9H9BrO3, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
Methyl 2-bromo-4-methoxybenzoate(45 mg, 1.4 equiv), BINAP (50 mg, 0.08 equiv), Pd (OAc) 2 (11.2 mg, 0.05 equiv) ), Toluene 20mL, N2 protection, 110 , the reaction 18h, filtered and the solvent was recovered, column chromatography to give a solid 165mg, yield 57%.
The synthetic route of 17100-65-1 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; Fudan University; Shanghai Jiao Tong University; He Qiuqin; Yin Ming; Fan Renhua; Han Dandan; Zhou Kaiyi; Song Runzhe; Zhao Lu; (11 pag.)CN107056702; (2017); A;,
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