Murray, Stephen published the artcileDirect derivatization of sulfate esters for analysis by gas chromatography mass spectrometry, Synthetic Route of 6217-68-1, the publication is Biomedical Mass Spectrometry (1979), 6(2), 82-9, database is CAplus.
Gas chromatog.-mass spectrometry was used to study the reaction between 13 aromatic, steroidal and aliphatic sulfate esters and 3 perfluoroacylating reagents, viz. (CF3CO)2O, (C2F5CO)2O and (CF3CF2CF2CO)2O. Aromatic sulfates reacted readily with 1:1 anhydride:AcOEt to give the perfluoro ester of the parent phenol quant. Nonaromatic sulfates gave a variety of products. A mechanism is proposed for the 1-step derivatization of aromatic sulfates, and the potential of the procedure for the anal. of sulfate conjugates by mass spectrometry is discussed.
Biomedical Mass Spectrometry published new progress about 6217-68-1. 6217-68-1 belongs to esters-buliding-blocks, auxiliary class Salt,Nitro Compound,Sulfonate,Benzene, name is Potassium 4-nitrophenyl sulfate, and the molecular formula is C6H4KNO6S, Synthetic Route of 6217-68-1.
Referemce:
https://en.wikipedia.org/wiki/Ester,
Ester – an overview | ScienceDirect Topics