Authors Wang, JJ; Jiang, F; Tao, CF; Yu, H; Ruhlmann, L; Wei, YG in ROYAL SOC CHEMISTRY published article about DEHYDROGENATION; EFFICIENT in [Wang, Jingjing; Jiang, Feng] Gannan Med Univ, Key Lab Cardiovasc & Cerebrovasc Dis Prevent & Co, Minist Educ, Ganzhou 341000, Jiangxi, Peoples R China; [Wang, Jingjing; Ruhlmann, Laurent] Univ Strasbourg, Inst Chim, Lab Electrochim & Chim Phys Corps Solide, UMR CNRS 7177, 4 Rue Blaise Pascal,CS 90032, F-67081 Strasbourg, France; [Tao, Chaofu; Yu, Han] Shanghai Inst Technol, Sch Chem & Environm Engn, Shanghai 201418, Peoples R China; [Yu, Han; Wei, Yongge] Tsinghua Univ, Dept Chem, Key Lab Organ Optoelect & Mol Engn, Minist Educ, Beijing 100084, Peoples R China; [Yu, Han; Wei, Yongge] Peking Univ, State Key Lab Nat & Biomimet Drugs, Beijing 100191, Peoples R China in 2021.0, Cited 19.0. Recommanded Product: 103-25-3. The Name is Methyl 3-phenylpropionate. Through research, I have a further understanding and discovery of 103-25-3
The direct esterification of alcohols with non-noble metal-based catalytic systems faces great challenges. Here, we report a new chrome-based catalyst stabilized by a single pentaerythritol decorated Anderson-type polyoxometalate, [N(C4H9)(4)](3)[CrMo6O18(OH)(3)C{(OCH2)(3)CH2OH}], which can realize the efficient transformation from alcohols to esters by H2O2 oxidation in good yields and high selectivity without extra organic ligands. A variety of alcohols with different functionalities including some natural products and pharmaceutical intermediates are tolerated in this system. The chrome-based catalyst can be recycled several times and still keep the original configuration and catalytic activity. We also propose a reasonable catalytic mechanism and prove the potential for industrial applications.
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Reference:
Patent; SANOFI; US2011/294788; (2011); A1;,
Ester – Wikipedia,
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