Application In Synthesis of Methyl 3-phenyl-2-propenoate. Recently I am researching about WATER-GAS SHIFT; ACID-CATALYZED DEPOLYMERIZATION; ANISOLE DECOMPOSITION; RHODIUM; ALKYLATION; MECHANISM; HYDROGENOLYSIS; TRANSFORMATION; ETHYLTOLUENE; EFFICIENT, Saw an article supported by the National Natural Science Foundation of ChinaNational Natural Science Foundation of China (NSFC) [21871277, 21703258]; Beijing Municipal Science & Technology CommissionBeijing Municipal Science & Technology Commission [Z1811000042180042]. Published in ROYAL SOC CHEMISTRY in CAMBRIDGE ,Authors: Shen, XJ; Meng, M; Mei, QQ; Xiang, JF; Liu, HZ; Han, BX. The CAS is 103-26-4. Through research, I have a further understanding and discovery of Methyl 3-phenyl-2-propenoate
4-Ethyltoluene is a very valuable chemical that is currently produced from fossil feedstocks. Production of 4-ethyltoluene from renewable and cheap lignin is of great significance. Herein, we report a new route to produce 4-ethyltoluene from lignin. It was discovered that RhCl3-LiI-LiBF4 was an efficient catalytic system for the reaction of lignin with CO to form 4-ethyltoluene. In the reaction, ethylbenzene was first formed via demethoxylation and depolymerization of lignin, which was further transformed into 4-ethyltoluene by methylation using methoxy from the lignin. The yield of 4-ethyltoluene could reach 9.5 wt% when GVL-lignin was used as the starting material. Interestingly, 5.2 wt% yield of 4-ethyltoluene was obtained when raw poplar was directly used as the starting material. As far as we know, the transformation of lignin with 4-ethyltoluene as the major product has not been reported. This work provides a new strategy to produce valuable aromatic compounds from renewable resources.
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Reference:
Article; Weng, Shiue-Shien; Ke, Chih-Shueh; Chen, Fong-Kuang; Lyu, You-Fu; Lin, Guan-Ying; Tetrahedron; vol. 67; 9; (2011); p. 1640 – 1648;,
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