Safety of Methyl 3-phenylpropionate. In 2019.0 ADV SYNTH CATAL published article about SILANE-REDUCTION; HECK REACTIONS; PALLADIUM; CLEAVAGE; CLUSTER; POLYMERIZATION; ALDEHYDES; REMOVAL in [Ikeda, Takuya; Zhang, Zhenzhong; Motoyama, Yukihiro] Toyota Technol Inst, Dept Adv Sci & Technol, Nagoya, Aichi 4688511, Japan in 2019.0, Cited 22.0. The Name is Methyl 3-phenylpropionate. Through research, I have a further understanding and discovery of 103-25-3.
Combination of PdCl2 with 1,1,3,3-tetramethyldisiloxane in the presence of activated carbon was found to be an effective catalyst system for the cleavage reaction of C-O bond of O-t-Bu moieties. The present catalytic reaction offers a practical method for the deprotection of tert-butyl esters, tert-butyl ethers, O-Boc, and N-Boc derivatives under mild conditions. The addition of activated carbon in the reaction mixture was proved to be crucial for not only sustaining the catalytic activity but also trapping the palladium species after the reaction.
Safety of Methyl 3-phenylpropionate. About Methyl 3-phenylpropionate, If you have any questions, you can contact Ikeda, T; Zhang, ZZ; Motoyama, Y or concate me.
Reference:
Patent; SANOFI; US2011/294788; (2011); A1;,
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