Reference of 88709-17-5, Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 88709-17-5, name is Ethyl 2-ethoxy-4-methylbenzoate, This compound has unique chemical properties. The synthetic route is as follows.
To a solution of ethyl 2-ethoxy-4-methylbenzoate 117 (10.0 g, 48.1 mmol) in a mixture of pyridine (25 mL) and water (75 mL) was added KMn04 (22.8g, 144.2 mmol). The resulting mixture was heated at 50 C for 48 hours, then cooled and allowed to stir at room (0540) temperature for 24 hours. The mixture was filtered and the filter cake washed with hot water. The combined aqueous filtrates were washed with EtOAc (75 mL x 3) and acidified with 2M aqueous HCI solution. The mixture was extracted with CH2CI2 (150 mL x 3). The combined organic layers were washed with brine, dried (Na2S04), filtered and concentrated to give the desired compound as a white solid (5.0 g, 44%): LCMS: RT 0.25 min; m/z 239.0 [M+H]+.
The chemical industry reduces the impact on the environment during synthesis Ethyl 2-ethoxy-4-methylbenzoate. I believe this compound will play a more active role in future production and life.
Reference:
Patent; CTXT PTY LIMITED; STUPPLE, Paul Anthony; (88 pag.)WO2017/153519; (2017); A1;,
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