Synthetic Route of 26759-46-6, A common heterocyclic compound, 26759-46-6, name is Methyl 2-amino-4,5-dimethoxybenzoate, molecular formula is C10H13NO4, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
General procedure: A mixture of 1a,b (10 mmol) and methyl 2-amino-4,5-dimethoxybenzoate (12 mmol, 2.52 g), freshly prepared fused sodium acetate (0.3 g) was heated in a boiling water bath in glacial acetic acid (10 mL) for 3 h. The crystalline product separated on cooling was filtered, washed with water, dried, and recrystallized from ethanol.
The synthetic route of 26759-46-6 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Georgey, Hanan; Molecules; vol. 19; 3; (2014); p. 3777 – 3792;,
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