Related Products of 2065-23-8, These common heterocyclic compound, 2065-23-8, name is Methyl 2-phenoxyacetate, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
To the methyl phenoxyacetate obtained by distillation, 1.72 g of tin tetrachloride having a purity of 99% and 0.60 g of 2,5-dichlorothiazole having a purity of 99% were added.279.41 g of 99% pure sulfuryl chloride was added at 60 C to react.After the addition, the reaction was kept at this temperature for 0.5 h.Distilling at a pressure of 1 kPa and collecting fractions at 115-125 C,234.12 g of methyl 2,4-dichlorophenoxyacetate was obtained, and the content was 99.18%.
Statistics shows that Methyl 2-phenoxyacetate is playing an increasingly important role. we look forward to future research findings about 2065-23-8.
Reference:
Patent; Shandong Runbo Biological Technology Co., Ltd.; Sun Guoqing; Hou Yongsheng; Chi Zhilong; Zhang Liguo; Hu Yishan; (15 pag.)CN108947822; (2018); A;,
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