Related Products of 63106-93-4, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 63106-93-4, name is 1-Phenyl-3-oxabicyclo[3.1.0]hexan-2-one belongs to esters-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
Step-2: Synthesis of compound 5: 5 [001.0].) 34 g of aluminium cbioride (0.255 moles) are suspended in 240 ml of toluene and then 38,3 g of diethylamine 4 (0.523 moles) are added while maintaining the temperature between 15 and 30C. The lactone 3 concentrate (38 g) obtained earlier step was poured into the reaction medium maintained at 2SQC. The reaction medium was stirred for at least 1 hour 30 minutes. Formation of a precipitate was observed. The reaction medium was hydro y zed with 345 mi of water and then filtered after adding a filtration adjuvant. After decantation, the organic phase was washed twice with 235 ml and 175 m of water and then concen trated to obtain the amide-alcohol intermediate 5.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1-Phenyl-3-oxabicyclo[3.1.0]hexan-2-one, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; KANDULA, Mahesh; WO2013/168002; (2013); A1;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics