Synthetic Route of 2065-23-8, The chemical industry reduces the impact on the environment during synthesis 2065-23-8, name is Methyl 2-phenoxyacetate, I believe this compound will play a more active role in future production and life.
167.87 g of 99% methyl phenoxyacetate (1 mol), 1.26 g of 99% zinc chloride and 1.68 g of 99% were sequentially added to a 500 mL four-necked flask.2,5-dichlorothiazole, 154.69 g of 99% chlorine (2.16 mol) was introduced at -20 C.After the heat preservation reaction for 30 minutes,Distilling and collecting fractions of 140-150 C under a pressure of 1 kpa,Methyl 2,4-dichlorophenoxyacetate236.21g, content 98.8%,The yield was 99.28% based on methyl phenoxyacetate.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, Methyl 2-phenoxyacetate, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Shandong Runbo Biological Technology Co., Ltd.; Sun Guoqing; Hou Yongsheng; Zhang Liguo; Chi Zhilong; Hu Yishan; (12 pag.)CN108947807; (2018); A;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics