Share a compound : Diethyl malonate

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 105-53-3, name is Diethyl malonate, This compound has unique chemical properties. The synthetic route is as follows., Computed Properties of C7H12O4

Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 105-53-3, name is Diethyl malonate, This compound has unique chemical properties. The synthetic route is as follows., Computed Properties of C7H12O4

General procedure: The respective aldehyde (1-8) (5 mmol) and diethyl malonate(9) (5 mmol) were added in the presence of piperidine (4 mmol)under an inert atmosphere and transformed into a viscous solution. It was refluxed for 5-6 h and quenched with 6 N HCl in cold conditions. The product was extracted with ethyl acetate(3 10 mL). The combined organic extracts were dried and evaporatedunder reduced pressure. Compounds (10-17) were recrystallized from 50% aqueous ethanol and carried forward without further purification.

According to the analysis of related databases, 105-53-3, the application of this compound in the production field has become more and more popular.

Reference:
Article; Shrivastava, Sushant K.; Srivastava, Pavan; Bandresh, Robin; Tripathi, Prabhash Nath; Tripathi, Avanish; Bioorganic and Medicinal Chemistry; vol. 25; 16; (2017); p. 4424 – 4432;,
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