Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 13831-03-3, name is tert-Butyl propiolate, A new synthetic method of this compound is introduced below., Quality Control of tert-Butyl propiolate
General procedure: Into an oven-dried reaction flask under Ar gas protection was added oxabicyclic alkene (0.2 mmol), Au catalyst (0.001 mmol), methyl propiolate (0.4 mmol) and toluene (1.0 mL). The reaction mixture was stirred at room temperature normally overnight. After complete consumption of the starting materials, monitored by TLC, the solvent was removed under reduced pressure and the residue was purified by flash column chromatography.
The synthetic route of 13831-03-3 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Sun, Yin-Wei; Xu, Qin; Shi, Min; Beilstein Journal of Organic Chemistry; vol. 9; (2013); p. 1969 – 1976;,
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