Application of 252881-74-6, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 252881-74-6, name is tert-Butyl 3-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)propanoate belongs to esters-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
Into a 10 liter glass reactor, 2080 g of a yellow oily liquid obtained in the above step and 4L of a 6 M hydrochloric acid solution were added. The reaction was carried out for 3 h at room temperature, and HPLC detection showed that the starting material had reacted completely. The reaction mixture was concentrated to dryness, neutralized with 1M sodium hydroxide solution to neutral, and concentrated again to dryness, samples were dissolved in dichloromethane, dried over anhydrous sodium sulfate, filtered, and concentrated to dryness to give a colorless oil 1650g. HPLC analysis showed a product purity of 97% and a total reaction yield of 91%
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, tert-Butyl 3-(2-(2-(2-aminoethoxy)ethoxy)ethoxy)propanoate, other downstream synthetic routes, hurry up and to see.
Reference:
Patent; Jiangsu Jinsirui Biological Technology Co., Ltd.; Shen Junwei; Zhang Fangliang; Zhang Jianqi; Luo Fulin; (11 pag.)CN109096128; (2018); A;,
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