Synthetic Route of 2672-58-4,Some common heterocyclic compound, 2672-58-4, name is Trimethyl benzene-1,3,5-tricarboxylate, molecular formula is C12H12O6, traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
To a solution of Trimethyl 1,3,5-Benzenetricarboxylate (1.1 g, 4.36 mmol) in MeOH (100 mL) wasadded 1 M NaOH aq. (3.95 mL, 3.95 mmol). The solution was stirred for 22 h at rt. After removal ofthe solvent by evaporation, the mixture was washed with CH2Cl2. The aqueous layer was acidified with 6 M HCl to pH 2 and then extracted with AcOEt. The organic layer was dried over Na2SO4 andthe solution was concentrated by evaporation to give 17 (849 mg, 79%) as a white solid.
The synthetic route of 2672-58-4 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Zenmyo, Naoki; Tokumaru, Hiroki; Uchinomiya, Shohei; Fuchida, Hirokazu; Tabata, Shigekazu; Hamachi, Itaru; Shigemoto, Ryuichi; Ojida, Akio; Bulletin of the Chemical Society of Japan; vol. 92; 5; (2019); p. 995 – 1000;,
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