Synthetic Route of 93-92-5, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 93-92-5, name is 1-Phenylethyl acetate belongs to esters-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
General procedure: A mixture of ester (1 mmol) and PBNS (30 mg) in H2O(2 mL) was stirred at ambient temperature. After completion of the reaction as monitored by TLC, the insoluble catalyst was separated by filtration. Water was removed by rotary evaporation and the residue was extracted with ethyl acetate(310 mL). The organic layer was dried over anhydrous Na2SO4. After evaporation of the solvent, the products were purified by column chromatography. The product?s purity was checked by TLC, it showed single spot of the final product, and evaporation of the solvent gave the desired pure products in good yields.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, 1-Phenylethyl acetate, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Khazaei, Ardeshir; Saednia, Shahnaz; Roshani, Liela; Kazem-Rostami, Masoud; Zare, Abdolkarim; Letters in Organic Chemistry; vol. 11; 3; (2014); p. 159 – 167;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics