Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 431-47-0, name is Methyl 2,2,2-trifluoroacetate, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 431-47-0
Trifluoroacetanilide (100 mg, 0.46 mmol), DMF (4 mL), potassium t-butoxide (153 mg, 1.37 mmol, 3 eq.) was added to the reaction mixture in turn, and stirred at room temperature for 5 minutes.After the potassium tert-butoxide was uniformly dispersed, methyl trifluoroacetate (0.19 mL, 1.84 mmol, 4 eq.) was slowly injected into the reaction flask, and after stirring at 60 C for 10 hours, stirring was stopped.Extract twice with ethyl acetate and distilled water, then wash with saturated NaCl solution.The organic phases were combined, and the organic phase was dried over anhydrous magnesium sulfate.Magnesium sulfate was removed by filtration, and the solvent was evaporated to give purified N-(4-methoxyphenyl)-N-methyltrifluoroacetamide (88 mg, yield 83%).
According to the analysis of related databases, 431-47-0, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Guangdong Petrochemical College; Xiao Duoduo; Zheng Xin; Zeng Jiechun; Huang Jiawei; Zhou Rujin; Guan Ying; Liang Jieling; (8 pag.)CN109369506; (2019); A;,
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