Continuously updated synthesis method about 2065-23-8

Application of 2065-23-8, The chemical industry reduces the impact on the environment during synthesis 2065-23-8, name is Methyl 2-phenoxyacetate, I believe this compound will play a more active role in future production and life.

Application of 2065-23-8, The chemical industry reduces the impact on the environment during synthesis 2065-23-8, name is Methyl 2-phenoxyacetate, I believe this compound will play a more active role in future production and life.

167.87 g of 99% methyl phenoxyacetate (1 mol), 1.26 g of 99% zinc chloride and 1.68 g of 99% 2,4,6-trimethyldiphenyl sulfide were successively added to a 500 mL four-necked flask.154.69g of 99% chlorine gas (2.16mol) was introduced at -20 C, and the reaction was allowed to stand for 30 min, and the fraction of 140-150 C was distilled under a pressure of 1 kpa to obtain methyl 2,4-dichlorophenoxyacetate. 236.21 g, content 98.8%, yield 99.28% based on methyl phenoxyacetate.

In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, Methyl 2-phenoxyacetate, other downstream synthetic routes, hurry up and to see.

Reference:
Patent; Shandong Runbo Biological Technology Co., Ltd.; Sun Guoqing; Hou Yongsheng; Zhang Liguo; Chi Zhilong; Hu Yishan; (14 pag.)CN108947821; (2018); A;,
Ester – Wikipedia,
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