Introduction of a new synthetic route about Methyl methylcarbamate

Application of 6642-30-4, A common heterocyclic compound, 6642-30-4, name is Methyl methylcarbamate, molecular formula is C3H7NO2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

Application of 6642-30-4, A common heterocyclic compound, 6642-30-4, name is Methyl methylcarbamate, molecular formula is C3H7NO2, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.

EXAMPLE 10 2-SEC BUTYLPHENYL N-METHYLCARBAMATE To a mixture of methyl N-methylcarbamate (0.89 g, 0.01 mole) and 2-sec butylphenol (1.5 g, 0.01 mole) in dichloroethane (10 ml), a solution of phosphorus tribromide (2.7 g, 0.01 mole) in dichloro-ethane (6 ml) was added and the mixture was refluxed for eight hours. It was then worked up and purified as described earlier to give 2-sec butylphenyl N-methylcarbamate of the formula (III).

The synthetic route of 6642-30-4 has been constantly updated, and we look forward to future research findings.

Reference:
Patent; Council of Scientific & Industrial Research; US5066819; (1991); A;,
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