In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 93-92-5, name is 1-Phenylethyl acetate belongs to esters-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. Recommanded Product: 1-Phenylethyl acetate
General procedure: A 1,2-dichloroethane (5.0mL) solution of isopropenyl acetate (2a) (0.3mmol), 1-phenylethyl acetate (10a) (0.3mmol) and ReBr(CO)5 was stirred under an atmosphere of nitrogen at 80C for 5h. After the reaction was complete, H2O was added to the reaction mixture and extracted with ethyl acetate. The organic layer was dried with MgSO4. The resulting mixture was filtered, and the filtrate was concentrated. Purification of the residue by silica gel column chromatography afforded 4-phenyl-2-pentanone (3a). The product (3a) was characterized by comparing its spectral data with those of authentic sample [23].
The synthetic route of 93-92-5 has been constantly updated, and we look forward to future research findings.
Reference:
Article; Umeda, Rui; Takahashi, Yuuki; Yamamoto, Takaaki; Iseki, Hideki; Osaka, Issey; Nishiyama, Yutaka; Journal of Organometallic Chemistry; vol. 877; (2018); p. 92 – 101;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics