Introduction of a new synthetic route about C8H14O2

These common heterocyclic compound, 4911-54-0, name is Ethyl 4-methylpent-4-enoate, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route. name: Ethyl 4-methylpent-4-enoate

These common heterocyclic compound, 4911-54-0, name is Ethyl 4-methylpent-4-enoate, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route. name: Ethyl 4-methylpent-4-enoate

EXAMPLE 13 The reaction is carried out as described in Example 8 but using catalyst 4a (7.6 mg, 0.01%) in THF (5 ml) and KOMe (0.63 g, 9 mmol) in ethyl 4-methylpent-4-enoate 11 (12.9 g, 91 mmol) and THF (58 ml). Standard work-up gave a slightly yellow crude oil (5.6 g, 61%) which contained 4-methyl pent-4-en-1-ol 12 of 100% purity according to GC. The analytical data of 4-methylpent-4-en-1-ol 12 were identical with the ones obtained from commercial samples of this compound.

The synthetic route of Ethyl 4-methylpent-4-enoate has been constantly updated, and we look forward to future research findings.

Reference:
Patent; Geisser, Roger Wilhelm; Goeke, Andreas; Schroeder, Fridtjof; US2015/152029; (2015); A1;,
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