Reference of 23676-08-6, These common heterocyclic compound, 23676-08-6, name is Methyl 4-ethoxybenzoate, its traditional synthetic route has been very mature, but the traditional synthetic route has various shortcomings, such as complicated route, low yield, poor purity, etc, below Introduce a new synthetic route.
General procedure: 4-dodecyloxy methylbenzoate(13.3 g, 0.04mol)was placed in a one liter single-necked round-bottom flask equippedwith double wall water condenser. Ethanol (250 ml) and potassium hydroxide (6 g, 0.1 mol)dissolved in distilled water (250 ml) were added to the flask. The solution was refluxed for2 hours and allowed to cool down at r.t. and then neutralized with 10% hydrochloric acidto get a white precipitate. It was purified by recrystallizing from methanol.
Statistics shows that Methyl 4-ethoxybenzoate is playing an increasingly important role. we look forward to future research findings about 23676-08-6.
Reference:
Article; Reddy, M. Kesava; Reddy, K. Subramanyam; Prakash; Narasimhaswamy; Molecular Crystals and Liquid Crystals; vol. 582; 1; (2013); p. 1 – 14;,
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