Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 13380-85-3, name is Methyl 4-(hydroxymethyl)cyclohexanecarboxylate, A new synthetic method of this compound is introduced below., HPLC of Formula: C9H16O3
The compound represented by Formula (1-1-2), pyridine, anddichloromethane were put into a reaction container under a nitrogen atmosphere. With ice cooling, methanesulfonyl chloride wasdropped, followed by stirring at room temperature. After ordinary post-treatment was performed, purification was performed by column chromatography (silica gel) to obtain a compound represented by Formula (1-1-3).
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Patent; DIC CORPORATION; TENG, Yan; HORIGUCHI, Masahiro; KADOMOTO, Yutaka; KOISO, Akihiro; HAYASHI, Masanao; SAITOU, Yoshitaka; LI, Zhimin; (201 pag.)WO2017/79867; (2017); A1;,
Ester – Wikipedia,
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