Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 10602-06-9, name is Methyl 3-ethynylbenzoate, This compound has unique chemical properties. The synthetic route is as follows., Recommanded Product: 10602-06-9
General procedure: CuCl (0.04 mmol), 2,4,6-trimethylpyridine (0.4 mmol), trifluoromethylating reagent 2a (0.24 mmol) and terminal alkynes (0.2 mmol) were added to a Schlenk tube which was equipped with a stirring bar. DMAc (1 mL) was added under argon atmosphere to this tube. After the addition of all materials, the reaction mixture was kept for 24 h at 30 C. After the reaction, ethyl acetate was added. The organic layer was separated, and washed with water. The combined organic extracts were washed with brine, and dried over MgSO4. After evaporation of the solvent, the crude product was purified by chromatography on silica gel to give the product.
According to the analysis of related databases, 10602-06-9, the application of this compound in the production field has become more and more popular.
Reference:
Article; Luo, Dong-Fen; Xu, Jun; Fu, Yao; Guo, Qing-Xiang; Tetrahedron Letters; vol. 53; 22; (2012); p. 2769 – 2772;,
Ester – Wikipedia,
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