Adding a certain compound to certain chemical reactions, such as: 6091-64-1, name is Ethyl 2-bromobenzoate, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 6091-64-1, COA of Formula: C9H9BrO2
General procedure: In a 10 mL schlenk tube with magnetic stirring bar, cercosporin(0.05 equiv), aryl halide 1 (0.2 mmol), arene 2 (20 equiv), DIPEA (4equiv) were dissolved in CH3CN (2 mL) and the resulting mixtures were placed under 23WCFL under N2 atmosphere. When the reaction was finished, the reaction mixture was washed with brine. The aqueous phase was reextracted with ethyl acetate. The combined organic extracts were dried over Na2SO4, concentrated in vacuum,and the resulting residue was purified by silica gel column chromatographyto afford the desired product 3.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, Ethyl 2-bromobenzoate, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Tang, Zhaocheng; Li, Jia; Lin, Fulin; Bao, Wenhao; Zhang, Shiwei; Guo, Baodang; Huang, Shuping; Zhang, Yan; Rao, Yijian; Journal of Catalysis; vol. 380; (2019); p. 1 – 8;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics