Each compound has different characteristics, and only by selecting the characteristics of the compound suitable for a specific situation can the compound be applied on a large scale. 6627-89-0, name is tert-Butyl phenyl carbonate, This compound has unique chemical properties. The synthetic route is as follows., name: tert-Butyl phenyl carbonate
1-(t-butoxycarbonyl)indole can be prepared according to the procedure described: D. Dhanak, C. B. Reese J. Chem. Soc., Perkin Trans. 1 1986, 2181-2186: sodium hydride, in suspension in mineral oil, (0.77 g, 25.6 mmol) is washed twice with pentane then put into suspension in 10 mL of THF under a nitrogen atmosphere at ambient temperature. A solution of indole (1.01 g, 8.6 mmol) in 8.2 mL of THF is then added to this suspension. Once the reaction is completed (release of H2), t-butyl and phenyl carbonate (2.0 g, 10.25 mmol) are then added dropwise. The resulting reaction mixture is stirred for a further period of 12 hours at ambient temperature. 15 mL of water are then added, then the resulting mixture is extracted 3 times with ether. The organic phase obtained is dried over anhydrous MgSO4, filtered then evaporated under vacuum. The residue is purified by distillation (boiling point: 84 C./0.25 mm Hg) in order to produce 1.465 g (78%). The spectral characteristics are described in the publication.
Chemical properties determine the actual use. Each compound has specific chemical properties and uses. We look forward to more synthetic routes in the future to expand reaction routes of 6627-89-0.
Reference:
Patent; UNIVERSITE JOSEPH FOURIER; CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; US2010/144726; (2010); A1;,
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