In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 2318-25-4, name is Ethyl 3-ethoxy-3-iminopropionate hydrochloride belongs to esters-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below. SDS of cas: 2318-25-4
Example P2: Preparation of Ethoxycarbonimidoyl-acetic acid ethyl ester. 25.7 g (0.131 mol) of ethoxycarbonimidoyl-acetic acid ethyl ester hydrochloride was suspended in 155 ml of dichlormethane and then a solution of 5.78 g (0.144 mol) of sodium hydroxide in 30 ml of water was added. After stirring for 30 min the layers were separated and the organics dried and vacced down to leave a colourless oil to give 19.35g of clean Ethoxycarbonimidoyl-acetic acid ethyl ester. 1H-NMR (CDCI3, ppm): 6.28 (s, br, 1 H), 4.19 (q, J=7 Hz, 2H), 4.02 (m, 2H), 3.37 (s, 1 H), 3.25 (s, 1 H), 1.30 (t, J=7Hz, 3H), 1.26 (t, J=7Hz, 3H).
The synthetic route of 2318-25-4 has been constantly updated, and we look forward to future research findings.
Reference:
Patent; SYNGENTA PARTICIPATIONS AG; SYNGENTA LIMITED; WO2008/6540; (2008); A1;,
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