Related Products of 606-45-1, In the next few decades, the world population will flourish. As the population grows rapidly and people all over the world use more and more resources, all industries must consider their environmental impact. 606-45-1, name is Methyl 2-methoxybenzoate belongs to esters-buliding-blocks compound, it is a common compound, a new synthetic route is introduced below.
In cyclohexane: To a suspension of AlI3 (5.5 mmol, 1.0 eq.) in cyclohexane (40 mL) was added methyl o-anisate (4, 0.915 g, 5.5 mmol). After stirring for 1 d under reflux, themixture was acidified with dilute HCl (2 M, 10 mL), extracted with EA (50 mL ¡Á 3). The combined organic phases were combined, washed with Na2S2O3, and dried over MgSO4.After filtration, the organic solvents were removed by a rotary evaporator, and the residue was purified through column chromatography (eluent: PE/EA 3:1) to afford 8 (0.661g, 86%) as a white solid.
In the field of chemistry, the synthetic routes of compounds are constantly being developed and updated. I will also mention this compound in other articles, Methyl 2-methoxybenzoate, other downstream synthetic routes, hurry up and to see.
Reference:
Article; Sang, Dayong; Yi, Cuicui; He, Zhoujun; Wang, Jiahui; Tian, Juan; Yao, Ming; Shi, Hong; Tetrahedron Letters; vol. 59; 15; (2018); p. 1469 – 1472;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics