Researchers who often do experiments know that organic synthesis is a process of preparing more complex target molecules from simple raw materials through one or more chemical reactions. Generally, it requires fewer steps, and cheap raw materials. 792-74-5, name is Dimethyl [1,1′-biphenyl]-4,4′-dicarboxylate, A new synthetic method of this compound is introduced below., Recommanded Product: 792-74-5
General procedure: To a solution of benzo[b]thiophene (8) (2.15g, 16.0mmol) in 20ml dry THF under an argon atmosphere at?30¡ãC, n-BuLi (10.0ml, 16.0mmol, 1.6M n-hexane) was added slowly. The mixture was treated with the corresponding ester and stirred at room temperature. After quenching with saturated aqueous NH4Cl-solution, the residue was extracted with CHCl3. The organic phase was dried (Na2SO4) and the solvent evaporated.
The basis of chemical reaction formula synthesis, the synthesis route is composed of some specific reactions and combined according to certain logical thinking. We look forward to the emergence of more reaction modes in the future.
Reference:
Article; Katzsch, Felix; Gruber, Tobias; Weber, Edwin; Journal of Molecular Structure; vol. 1114; (2016); p. 48 – 64;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics