The chemical industry reduces the impact on the environment during synthesis 1865-29-8, name is Methyl 2-phenylacrylate, I believe this compound will play a more active role in future production and life. 1865-29-8
A solution of LiAlD4 (95 mg, 2.3 mmol) and AlCl3 (100 mg, 0.75 mmol) in THF was allowed to stir for 10 minutes before the addition of ester 16 (120 mg, 0.74 mmol) in THF. After 1.5 hours, the solution was quenched by addition of H2O, extracted with ether, and the ether extracts were dried (MgSO4) and concentrated in vacuo. The resulting oil was purified via flash column chromatography (15% EtOAc in hexane) to give the desired product 19 as a white solid (35 mg, 35%).
The chemical industry reduces the impact on the environment during synthesis 1865-29-8. I believe this compound will play a more active role in future production and life.
Reference:
Article; Richardson, Rebekah M.; Barney, Rocky J.; Wiemer, David F.; Tetrahedron Letters; vol. 53; 49; (2012); p. 6682 – 6684;,
Ester – Wikipedia,
Ester – an overview | ScienceDirect Topics