Adding some certain compound to certain chemical reactions, such as: 178312-47-5, name is Ethyl 4,4-difluorocyclohexanecarboxylate, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 178312-47-5. 178312-47-5
Example 1 : 4,4-Difluorocyclohexanecarboxamide; A suspension of ethyl 4,4-difluorocyclohexanecarboxylate (2500mg, 13mmol) in ammonium hydroxide (28%, 50 ml) was stirred at 60 C overnight. After removal of solvent, the residue was washed with water. The precipitate was obtained as product (white solid, 800 mg). 1H NMR (300 MHz, CDCl3): delta 5.31-5.45 (br, 2H), 2.02-2.27 (m, 3H), 1.92-2.02 (m, 2H), 1.72- EPO
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