85-91-6, Adding a certain compound to certain chemical reactions, such as: 85-91-6, name is Methyl N-Methylanthranilate, belongs to esters-buliding-blocks compound, can increase the reaction rate and produce products with better performance than those obtained under traditional synthetic methods. Here is a downstream synthesis route of the compound 85-91-6.
A 500 mL three-necked flask was placed in an ice-water bath,36.21 g (0.25 mol) of calcium hypochlorite was added,Distilled water 150mL,Glacial acetic acid (36 mL),Ice water bath reaction to the solution showed light yellow,28.13 g (0.17 mol) of methyl o-methylbenzoate was slowly added,And acetone (100mL) mixture,Stir under ice-water bath for 2 hours.After completion of the reaction, 100 mL of distilled water was added,Extraction with ethyl acetate (100 mL x 4)The extracts were combined and the organic layer was washed with saturated NaHCO3 solution,Dried over anhydrous magnesium sulfate, filtered and concentrated to give 25.43 g of a dark brown liquid,No purification is required and used directly in the next step.
According to the analysis of related databases, 85-91-6, the application of this compound in the production field has become more and more popular.
Reference:
Patent; Lupanshui Normal College; Yang Dan; (22 pag.)CN106279046; (2017); A;,
Ester – Wikipedia,
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