927-68-4, The chemical industry reduces the impact on the environment during synthesis 927-68-4, name is 2-Bromoethyl acetate, I believe this compound will play a more active role in future production and life.
Step D2-azidoethyl acetateN3^0AC [00269] A mixture of 2-bromoethyl acetate (500 muIota, 4.54 mmol) in N,N-dimethylformamide (DMF) (2.0 mL) was treated with sodium azide (295 mg, 4.54 mmol) and then heated to 70 C for 2 hours. The mixture was diluted with water and then extracted with ether. The extracts were washed with water, then brine, dried over sodium sulfate, filtered and concentrated to afford the title compound as a colorless liquid. 1H NMR (400 MHz, CHLOROFORM-d) d = 4.29 – 4.19 (m, 2 H), 3.53 – 3.44 (m, 2 H), 2.1 1 (s, 3 H).
The chemical industry reduces the impact on the environment during synthesis 2-Bromoethyl acetate. I believe this compound will play a more active role in future production and life.
Reference:
Patent; GLAXOSMITHKLINE LLC; DE LA ROSA, Martha Alicia; HAYDAR, Simon, N.; JOHNS, Brian Alvin; VELTHUISEN, Emile Johann; WO2012/102985; (2012); A1;,
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